Chemistry 313 Preliminary Report on Grignard Synthesis Turn this page in on Thursday, March 14th. It will be returned the same day. Info on other side should be provided on March 19th with write-up.Name __________________________________________________ Alkyl or Aryl Halide: Structure ______________________________ Volume to be used _______________ Number of Moles _______________ Magnesium: Weight to be used _______________ Number of Moles _______________ Carbonyl Component: Structure ______________________________ Weight or volume to be used _______________ g or ml Number of Moles _______________ Diethyl Ether (Anhydrous): Volume used with: Rx ________________ ml Carbonyl Component __________________ ml Total Volume to be used _______________ ml Stucture of Product: ______________________________________________ Name of Product: ________________________________________________ Theoretical yield of product: _____________________________________ (g or ml) Write a balanced equation for the total Grignard synthesis using the reagents assigned to you. Literature Data on Product and Side Products: References to synthesis (if any) _______________________________________ ______________________________________ Product: Melting Point ____________ Boiling Point ____________ (pressure) Specific gravity ___________ Index of Refraction ________________ Reference for above information: _______________________________________ _______________________________________ Side Products: Structure(s): Physical constants of each: Literature references: (Give a separate reference for each side product).
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